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Sketch For An Experimental Setup For Sublimation

Sketch for an Experimental Setup for Sublimation

Introduction

Sublimation is the physical process in which a solid substance directly transforms/converts into the gas state without going through the liquid state. This phenomenon can be observed when a solid is heated to a temperature and pressure below its triple point, the temperature, and pressure at which the solid, liquid, and gas phases coexist in equilibrium.

Experimental Setup

  1. Materials:
    • Solid sample (e.g., dry ice, camphor, or naphthalene)
    • Vacuum chamber or desiccator
    • Vacuum pump
    • Thermometer
    • Pressure gauge
  2. Procedure:
    • Place the solid sample in a vacuum chamber or desiccator.
    • Connect the vacuum pump to the vacuum chamber and start the pump to reduce the pressure inside.
    • Monitor the temperature and pressure inside the chamber using the thermometer and pressure gauge.
    • Observe the physical changes of the solid sample as the pressure and temperature decrease.

Expected Results

As the pressure and temperature inside the vacuum chamber decrease, the solid sample will begin to sublime. The sublimation rate will increase as the pressure and temperature decrease further. The sublimed gas will condense on the walls of the vacuum chamber or desiccator.

Applications of Sublimation

Sublimation is used in various applications, including:
  • Purification of substances
  • Freeze-drying of food and pharmaceuticals
  • 3D printing
  • Production of nanomaterials

Conclusion

The experimental setup described in this article provides a simple and effective way to demonstrate the sublimation process. By understanding the principles of sublimation, scientists and engineers can develop and optimize various technologies and applications that utilize this phenomenon.


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